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Mitigating drying shrinkage and enhancing mechanical strength of fly ash-based geopolymer paste with functionalized MWCNTs ... 1 1 Introduction 1 2 Experimental programs 2 2.1 Raw materials 2 2.2 Preparation process of modified geopolymer 3 2.2.1 Preparation of silane coupling agent modified MWCNTs 4 2.2.2 Preparation of geopolymer pastes 4 2.3 Testing methods 5 2.3.1 Dispersibility characterization of MWCNTs in aqueous solution 5 2.3.2 Characterization of the geopolymer 5 2.3.3 Mechanical properties characterization method 5 2.3.4 Mass loss and shrinkage behavior characterization method 6 2.3.5 Mercury intrusion porosimetry(MIP) 6 2.3.6 29Si solid-state nuclear magnetic resonance(NMR) 6 3 Result and discussion 6 3.1 Dispersibility of modified MWCNTs 6 3.1.1 Structural characterization of the modified MWCNTs 6 3.1.2 Dispersibility of modified MWCNTs in aqueous solution 7 3.2 Reaction kinetics and reaction products 8 3.3 Mechanical strength 12 3.4 Drying shrinkage and mass loss 12 3.5 Pore size distribution 13 3.5.1 Critical pore size (ds) 14 3.5.2 Influence of ds on drying shrinkage 14 3.6 Microstructural rearrangement 15 4 The mechanism on decreasing drying shrinkage and enhancin

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