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Physical and chemical characterization of urban grime: An impact on the NO2 uptake coefficients and N-containing product c... 1 1. Introduction 2 2. Materials and methods 2 2.1. Sampling of urban grime 2 2.2. Characterization of the urban grime 2 2.2.1. Scanning electron microscopy 2 2.2.2. Elemental carbon (EC) and organic carbon (OC) 2 2.2.3. Water-soluble organic carbon (WSOC) 3 2.2.4. Ion analysis 3 2.2.5. Inductively coupled plasma mass spectrometer (ICP-MS) 3 2.2.6. Gas chromatography-mass spectrometry (GC–MS) measurements 3 2.3. Flow tube reactor 3 2.4. Secondary electrospray ionization high-resolution mass spectrometry (SESI-HRMS) 4 2.4.1. The double bond equivalent (DBE) and aromaticity equivalent (Xc) 4 3. Results and discussion 4 3.1. Ionic composition of urban grime 4 3.2. PAHs and n-alkanes 4 3.3. Surface chemical composition and physical analysis 6 3.4. Reactive uptake of NO2 on urban grime 6 3.5. Formation of HONO 7 3.6. Gas phase product compounds formed upon heterogeneous reaction of NO2 with urban grime 8 4. Conclusions 9 CRediT authorship contribution statement 10 Declaration of competing interest 10 Acknowledgments 10 Appendix A. Supplementary data 10 Reference
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