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The document discusses the cathodic reduction of 1-nitroalkenes to oximes and primary amines. 1-Nitroalkenes are reduced at mercury or graphite cathodes in high yields to oximes at -0.3 to -0.5 V, and to primary amines at -1.1 V. Nitroalkadienes are selectively reduced at the double bond conjugated to the nitro group to oximes or amines. Various 1-nitroalkene substrates are reduced to demonstrate the method.
- Author
- alchemy090909
- Language
- EN