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Reaction of Pentacarbonyl(triphenylstannyl)manganese with Tetraphenylcyclopentadienone by R.D. Gorsich is a Chemistry article available to read on EtoBox.
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## Reaction of pentacarbonyI(triphenyIstannyI)manganese with tetraphenylcyclopentadienone \_-dditional work has been done to elucidate the structure of the product2 obtained by heating pentacarbonyl(triphen~lstannyl)manganese, (I), and tetraphenylcyclopentadienone at 196'. Prex-iously-" the product was suggested to be dienone complex (II) with a Sn-Mn bond. 0-Sn Ph3 Re-interpretation of the infrared spectrum of the comples disclosed no keto carbonyl, and indicated the reaction involved more than simple displacement of carbon mono-side from manganese. Xow, by a chemical method, we have shown the compound formed in the thermal reaction actually is tricarbonvl[(triphenq-lstanno~~~tetraphenylq-clopentadienyl~ manganese, (III), an isomer of the previously reported compound(I1) \_ Xoreover, structure (III) has been substantiated by au X-ray diffraction stud\_v3\_ J\_ Orgaxometal.
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- Author
- R.D. Gorsich
- Publisher
- Elsevier Science; Elsevier ; Elsevier BV (ISSN 0022-328X)
- Published
- 1966
- Language
- EN
- Field
- Chemistry (Physical Sciences)