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generally destroys the biological tissue. Therefore, the dynamics of water and ice in biological and synthetic solutions has enormous importance in various technological, biological and basic research fields. In this work, we apply broadband dielectric spectroscopy combined with calorimetric measurements to elucidate the dynamics of water in aqueous solutions, where all the water was fully amorphous or partly crystalline. The crystallinity degree was obtained by performing different annealing at temperatures between the glass transition and the cold-crystallization. We elucidated how the dynamical behavior of the water is altered both during and after the annealing. For partially crystalline aqueous solutions, after the annealing, it was found that the amorphous water dynamics and glass transition temperature were affected by the crystallinity, but that these effects can almost completely be explained by freeze concentration of the solution. Thus, the water dynamics of the partially crystalline sample becomes the same as for a fully amorphous sample with the same water concentration as the amorphous part of the partially crystalline solution.

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Author

Janice De M.V. Vilela

Publisher

Elsevier BV

Published

2022

Language

EN

Field

Medicine (Health Sciences)